一.参数指标:
(1)气相部分:
1)气相色谱柱箱
① 操作温度:室温以上4℃到450℃
② 温度设定值分辨率:1℃
③ 最大升温速率:120℃/min
④ 最长运行时间:999.99分钟
⑤ 室温每变化1℃柱温变化:<0.0l℃
⑥ ★降温:450℃到50℃,<4分钟
⑦ 程序升温20阶,21个平台,可梯度降温
2)加热区
① 不包括柱箱的独立加热区:6个
② 辅助加热区最高使用温度:400℃
3)气路控制
① 多路电子压力控制(EPC),通道用于进样口、 检测器或辅助气路(如阀等)
② ★以0.l psi的增量调节压力(精度)
③ 大气压力传感器补偿高度或环境的变化
④ 程序升压/升流:3阶
⑤ 具有多种电子流量控制操作模式一恒流、恒压、程序升流、程序升压、脉冲压力
4)进样口
① 分流/不分流毛细管柱进样口
② 最高使用温度400℃
③ 压力设定范围:0-150psi
④ 总流量设定范围:0-200m1/min N2;0-1000ml/min H2或He
5)自动进样系统
① 自动进样器:≥16位
② 自动进样重复精度:<1%
③ 进样量范围:0.1~50uL
④ 进样量线性:≥99%
(2)质谱检测器部分:
1) 离子源:惰性材料离子源
2) 离子化方式:EI
3) ▲质量分析器:四极杆质量分析器,带可拆卸的预四极过滤装置
4) 真空系统:大于等于60L/s的分子涡轮泵
5) 离子源温度:150-350℃
6) 接口温度范围:100-350℃
7) 质量范围:至少满足1.5-1050 amu
8) 质量轴稳定性:优于 0.10 amu/48 hrs
9) 分辨率:单位质量数分辨
10) 扫描速度:10000 amu/ s
11) 灵敏度:
① 全扫描(电子轰击源EI,m/z272): 5pg八氟萘(OFN),信/噪比≥150:1;
② 选择离子检测(电子轰击源EI,m/z272):500fg八氟萘,信/噪比≥150:1
12) 数据处理:
气相色谱,质谱,质谱工作站之间的数据传输全部依靠自身安装的网卡实现,具有网络通讯功能,可实现远程操作;手动/自动调谐;操作环境:Windows 2000 or XP;谱库:NIST谱库;中文软件系统:分为仪器控制、数据采集、数据处理和谱图检索四个功能模块。
二.气质联用仪配置单:
序号 |
名称 |
数量 |
备注 |
1. |
质谱主机 |
1台 |
—— |
2. |
前级真空泵 |
1台 |
—— |
3. |
涡轮分子泵 |
1个 |
PFEIFFER-VACUUM 包含在质谱主机中 |
4. |
离子源 |
1个 |
EI电离源 包含在质谱主机中 |
5. |
质量分析器 |
1台 |
四极杆质量分析器 包含在质谱主机中
|
6. |
检测器 |
1个 |
Detech电子倍增器 包含在质谱主机中 |
7. |
用户手册 |
1册 |
—— |
8. |
控制及数据处理软件(包括NIST库) |
1套 |
—— |
9. |
气相色谱 |
1台 |
Agilent7890 单分流/不分流进样口带EPC |
10. |
色谱使用说明光盘 |
1张 |
—— |
11. |
启动工具包 |
1套 |
包括工具、管路、气路 |
12. |
毛细管柱 |
1根 |
HP-5,30m x 0.32mm x 0.25um |
13. |
|
1台 |
Agilent 7693 、16位 |
14. |
耗材包 |
1套 |
含少量进样隔垫、衬管等耗材;如果需要增加,需另外购买 |
15. |
合格证 |
1张 |
—— | |
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GC-MS Agilent7890 +M7
Product Description A. Parameter index: (1) Gas parts: 1) gas column box ① Operating temperature: room temperature for more than 4 ℃ to 450 ℃ ② Temperature settings Resolution: 1 ℃ The ③ maximum heating rate: 120 ℃ / min ④ the longest running time: 999.99 minutes ⑤ room temperature changes every 1 ° C column temperature changes: <0.0l ℃ ⑥ ★ cooling: 450 ℃ to 50 ℃, <4 minutes ⑦ temperature programmed for 20 bands, 21 platform gradient cooling 2) the heating zone (1) does not include independent heating zones of the oven: 6 ② auxiliary heating maximum temperature: 400 ℃ 3) pneumatic control ① multi-channel electronic pressure control (EPC), the channel used for the inlet, detector or auxiliary gas (such as valves, etc.) ② ★ 0.l psi increments to adjust the pressure (accuracy) ③ changes in atmospheric pressure sensors compensate for height or environment (4) procedures for boost / l flow: order ⑤ with a variety of electronic flow control mode of operation, a constant current, constant voltage, the program up-flow procedures boost the pulse pressure 4) Inlet ① split / splitless capillary column inlet The ② maximum use temperature of 400 ℃ (3) pressure setting range :0-150psi ④ the total flow setting range :0-200m1 / min, N2,; 0-1000ml/min H2 or He 5) autosampler system ① autosampler: ≥ 16-bit ② autosampler Repeatability: <1% ③ Injection range: 0.1 ~ 50uL ④ the injection volume was linear: ≥ 99% (2) mass spectrometry detector part: 1) ion source: inert material ion source 2) ionization mode: EI 3) ▲ mass analyzer: four pre-quadrupole mass analyzer with a detachable four pole filter device 4) Vacuum system: greater than or equal to 60L / s turbo-molecular pump 5) The ion source temperature :150-350 ℃ 6) Interface temperature range :100-350 ° C 7) quality: at least 1.5-1050 amu 8) Mass axis stability: Better than 0.10 amu/48 hrs 9) Resolution: the number of unit mass resolution Scanning speed of 10): 10000 amu / s 11) Sensitivity: ① full scan (electron bombardment source EI m/z272): 5 pg OFN (OFN), signal / noise ratio ≥ 150:1; ② selected ion monitoring (electron impact source EI m/z272): 500fg eight fluorine naphthalene signal / noise ratio ≥ 150:1 12) data processing: Gas chromatography, mass spectrometry, mass spectrometry workstation data transfer between all rely on their own installation of NICs to achieve, with a network communication function can be performed remotely; manual / automatic tuning; operating environment: Windows 2000 or XP; spectral libraries: NIST spectral library; Chinese software systems: divided into instrument control, data acquisition, data processing and spectrum to retrieve the four functional modules. Two. GC single instrument configuration: Description Qty Remarks Mass spectrometry host 1 - (2) pre-vacuum pump 1 set - (3) a turbo-molecular pump PFEIFFER-VACUUM is included in the mass spectrometry host An EI ionization source (4) ion source is included in the MS host Mass analyzer quadrupole mass analyzer is included in the mass spectrometry host 6. Detector 1 Detech electronic multiplier included in the MS host 7 user manual 1 - 8 control and data processing software (NIST library) 1 set - Gas chromatography 1 Agilent7890 single split / splitless inlet with EPC 10 chromatography using CD for 1 - 11 Start Kit 1 set including tools, pipes, gas 12 capillary column, a HP-5, 30m x 0.32mm x 0.25um 13 automatic liquid sampler 1 Agilent 7693, 16-bit 14. Supplies package sets containing a small amount of the injection septum, liner and other supplies; If you need to increase, sold separately 15 certificate 1 -
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